Practical Organic Chemistry for Advanced Students

acetic acid acetyl chloride action added aldehyde aliphatic alkaline alkyl amines ammonia ammonium anhydride aniline apparatus aqueous aromatic benzaldehyde benzene benzyl benzyl chloride boiling bromine bulb c.c. of water c.c. water calcium chloride carbon caustic potash caustic soda cold water colour Colourless liquid combustion tube compound conc cooling cork crystallises crystals cyanide decanted decomposed dilute dimethylaniline dioxide dissolved distilled distilling flask drops ester ether ethyl ethyl acetate filtered filtrate flame formed fuming glass glycerin grams grms H₂O halogen heated hot water hour hydrocarbon hydrochloric acid hydrogen iodide ketones layer litre mixture nitric acid nitrobenzene obtained phenol phenylhydrazine phosphorus potassium poured powdered precipitate Prep PREPARATION Properties reaction residue retort round flask salt separated shaking shown in Fig small quantity smell sodium nitrite soluble in water substance sulphate sulphonic sulphuric acid tap-funnel temperature test-tube thermometer upright condenser warm washed water-bath whilst yellow Yield دو